Publications of the Chemistry Department

Publications of the BIPM Chemistry Department

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Clin. Chem. Lab. Med. 61 (2023) 1558-1560

Implementing metrological traceability of C-reactive protein measurements: consensus summary from the Joint Committee for Traceability in Laboratory Medicine Workshop

Pure and Applied Chemistry 95 (2023) 1-77

Methods for the SI-traceable value assignment of the purity of organic compounds (IUPAC Technical Report)


Steven Westwood, Katrice Lippa, Yoshitaka Shimuzu, Beatrice Lalerle, Takeshi Saito, David Duewer, Xinhua Dai, Stephen Davies, Marina Ricci, Annarita Baldan, Brian Lang, Stefan Sarge, Haifeng Wang, Ken Pratt, Ralf Josephs, Mikael Mariassy, Dietmar Pfeifer, John Warren, Wolfram Bremser, Stephen Ellison, Blaza Toman, Michael Nelson, Ting Huang, Ales Fajgelj, Ahmet Gören, Lindsey Mackay, Robert Wielgosz

Anal. Bioanal. Chem. (2022) 791-806

Metrological framework to support accurate, reliable, and reproducible nucleic acid measurements


Milavec M., Cleveland M.H., Bae Y.-K., Wielgosz R.I., Vonsky M., Huggett J.F.

Clin. Chem. Lab. Med. 61 (2022) 48-54

Overcoming challenges regarding reference materials and regulations that influence global standardization of medical laboratory testing results.

Anal. Bioanal. Chem. (2021) 1861-1870

Structurally related peptide impurity identification and accurate quantification for synthetic oxytocin by liquid chromatography–high-resolution mass spectrometry

Meas. Sci. Technol. 33 (2021) 014003

qNMR characterization of potential peptide calibrators for isotope dilution LC–MS quantification of a SARS-CoV-2 IgG monoclonal antibody

J. AOAC Int. 102 (2019) 1740-1748

The BIPM Mycotoxin Metrology Capacity Building and Knowledge Transfer Program: Accurate Characterization of a Pure Aflatoxin B1 Material to Avoid Calibration Errors

Elem. Sci. Anth. 7 (2019) 28

Stability of gaseous volatile organic compounds contained in gas cylinders with different internal wall treatments


Rhoderick G.C., Cecelski C.E., Miller W.R., Worton D.R., Moreno S., Brewer P.J., Viallon J., Idrees F., Moussay P., Kim Y.D., Kim D., Lee S., Baldan A., Li J.

TrAC-Trend. Anal. Chem. (2018) 108-119

State-of-the-art and trends for the SI traceable value assignment of the purity of peptides using the model compound angiotensin

Anal. Bioanal. Chem. (2018) 1-12

Identification and accurate quantification of structurally related peptide impurities in synthetic human C-peptide by liquid chromatography-high resolution mass spectrometry

Anal. Bioanal. Chem. 409 (2017) 2559-2567

Impurity determination for hepcidin by liquid chromatography - high resolution and ion mobility mass spectrometry for the value assignment of candidate primary calibrators


Bros P., Josephs R.D., Stoppacher N., Cazals G., Lehmann S., Hirtz C., Wielgosz R.I., Delatour V.

Anal. Chem. 89 (2017) 3648-3655

Calibration strategies for FT-IR and other isotope ratio infrared spectrometer instruments for accurate δ13C and δ18O measurements of CO2 in air


Flores E., Viallon J., Moussay P., Griffith D.W.T., Wielgosz R.I.

J. Chem. Metr. 11 (2017) 1-8

Concept Paper on SI Value Assignment of Purity - Model for the Classification of Peptide/Protein Purity Determinations.


Josephs R.D., Stoppacher N., Westwood S., Wielgosz R.I., Li M., Quaglia M., Melanson J., Martos G., Prevoo D., Wu L., Scapin S., Öztug Senal M., Wong L., Jeong J.-S., Chan K.W.Y., Arsene C.G., Park S.-R.

Clin. Chem. 63 (2017) 1447-1456

Implementing a reference measurement system for C-peptide: Successes and lessons learned

Proc. International School of Physics "Enrico Fermi" 196 (2017) 89-120

Comparisons of gas standards for climate change and air quality monitoring

Proc. International School of Physics « Enrico Fermi » 196 (2017) 121-147

Chemical primary reference materials: From valine to C-peptide

J Mol. Spectrosc. 327 (2016) 105-121

Absorption cross-sections of ozone in the ultraviolet and visible spectral regions: Status report 2015


Orphal J., Staehelin J., Tamminen J., Braathen G., De Backer M.-R., Bais A., Balis D., Barbe A., K. Bhartia P., Birk M., Burkholder J.B., Chance K., von Clarmann T., Cox A., Degenstein D., Evans R., Flaud J.-M., Flittner D., Godin-Beekmann S., Gorshelev V.

Anal. Chem. 87 (2015) 3272-3279

Methane standards made in whole and synthetic air compared by CRDS and GC-FID for atmospheric monitoring applications

Anal. Bioanal. Chem. 407 (2015) 3147–3157

Normal phase-liquid chromatography-tandem mass spectrometry with atmospheric pressure photoionization for the purity assessment of 17ß-estradiol

Rapid Comm. Mass Spectrom. 29 (2015) 1651-1660

Accurate quantification of impurities in pure peptide material – angiotensin I: Comparison of calibration requirements and method performance characteristics of liquid chromatography coupled to hybrid tandem mass spectrometry and linear ion trap-high

Appl. Spectrosc. 67 (2013) 1171-1178

Accurate Fourier transform infrared (FT-IR) spectroscopy measurements of nitrogen dioxide (NO2) and nitric acid (HNO3) calibrated with synthetic spectra

GAW Report No. 209 (2013) 76 pp

Guidelines for continuous measurements of ozone in the troposphere


Galbally I.E., Schultz M.G., Buchmann B., Gilge S., Guenther F., Koide H., Ottmans S., Patrick L., Scheel H.-E., Smit H., Steinbacher M., Steinbrecht W., Tarasova O., Viallon J., Volz-Thomas A., Weber M., Wielgosz R., Zellweger C.

J. Air & Waste Manage. Assoc. 63 (2013) 565-574

Temperature measurement and optical path-length bias improvement modifications to National Institute of Standards and Technology ozone reference standards

Anal. Bioanal. Chem. 405 (2013) 8039-8051

Impurity identification and determination for the peptide hormone angiotensin I by liquid chromatography–high-resolution tandem mass spectrometry and the metrological impact on value assignments by amino acid analysis

Anal. Chem. 85 (2013) 3118-3126

Mass balance method for the SI value assignment of the purity of organic compounds

Anal. Chem. 84 (2012) 10283-10290

Highly accurate nitrogen dioxide (NO2) in nitrogen standards based on permeation

J. Geophys. Res. 117 (2012)

Relative measurements of ozone absorption cross-sections at three wavelengths in the Hartley band using a well-defined UV laser beam

WMO/GAW Report No. 195 (2011) 47 pp

WMO/GAW Expert Workshop on Global Long-term Measurements of Nitrogen Oxides and Recommendations for GAW Nitrogen Oxides Network (October 2009)


Penkett S., Gilge S., Plass-Duelmer C., Galbally I., Brough N., Bottenheim J., Flocke F., Gerwig H., Lee J., Milton M., Rohrer F., Ryerson T., Steinbacher M., Torseth K., Wielgosz R.

J. Chromatogr. A (2010) 4535-4543

Simultaneous determination of various cardiac glycosides by liquid chromatography-hybrid mass spectrometry for the purity assessment of the therapeutic monitored drug digoxin

CHIMIA Int. J. Chem. (2009) 606-612

International activities in Metrology in Chemistry