CCM.FF-K4, EURAMET.M.FF-K4.b, SIM.M.FF-K4, and APMP.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 20 L
Degrees of equivalence Di and expanded uncertainty Ui at approximately 95% level of confidence, expressed in 10-6
Click on the Graph below to get a closer view and the names of the participating laboratories
Red diamonds : participants in CCM.FF-K4
Blue circles : participants in EURAMET.M.FF-K4.b
Green triangles : participants in SIM.M.FF-K4
Orange squares : participants in APMP.M.FF-K4
CCM.FF-K4 and SIM.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 100 mL
TRANSFER STANDARD: TS 03.04.04
Degrees of equivalence Di and expanded uncertainty Ui at approximately a 95% level of confidence
Red diamonds : participants in CCM.FF-K4
Green triangles : participants in SIM.M.FF-K4
DBSJ = 10601 x 10-6
UBSJ = 721 x 10-6
CCM.FF-K4, EURAMET.M.FF-K4.b, SIM.M.FF-K4, and APMP.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 20 L
Full set of degrees of equivalence relative to the CCM.FF-K4 key comparison reference value
In Red: participants in CCM.FF-K4
In Blue: participants in EURAMET.M.FF-K4.b
In Green: participants in SIM.M.FF-K4
In Orange: participants in APMP.M.FF-K4
Matrix of equivalence for key comparisons CCM.FF-K4 and EURAMET.M.FF-K4.b
Note: Pair-wise degrees of equivalence involving CCM.FF-K4 and SIM.M.FF-K4 are given on page 16 of the SIM.M.FF-K4 Final Report.
Pair-wise degrees of equivalence involving APMP.M.FF-K4 participants are given on page 17 of the APMP.M.FF-K4 Final Report.
| Lab i | Di | Ui |
| / 10-6 | / 10-6 | |
| CENAM | -3 | 15 |
| NIST | -26 | 34 |
| NRC | 13 | 30 |
| SP | 0 | 34 |
| PTB | -1 | 19 |
| INRIM | 24 | 16 |
| NMIA | -5 | 21 |
| INMETRO | -3 | 14 |
| SP* | 9 | 31 |
| JV* | 30 | 44 |
| METAS* | -66 | 64 |
| IPQ* | 10 | 35 |
| VSL* | -10 | 40 |
| SMU* | -27 | 27 |
| MKEH* | 3 | 26 |
| INRIM* | -7 | 27 |
| PTB* | -11 | 27 |
| DMDM* | -11 | 39 |
| UME* | -2 | 27 |
| EIM* | -16 | 25 |
| BEV* | -8 | 30 |
| CMI* | -66 | 89 |
* participants in EURAMET.M.FF-K4.b
Results are presented under A4 printable format in Summary Results (.PDF file).
CCM.FF-K4 and SIM.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 100 mL
TRANSFER STANDARD: TS 03.04.04
| Lab i | Di | Ui |
| / 10-6 | / 10-6 | |
| CENAM | -5 | 15 |
| NRC | 37 | 20 |
| SP | 13 | 27 |
| INRIM | -21 | 21 |
| NMIA | 10 | 19 |
| INMETRO | -14 | 17 |
| CENAM* | -3 | 22 |
| BSJ* | 10601 | 721 |
| LACOMET* | 13 | 64 |
| CENAMEP AIP* | -15 | 32 |
| INDECOPI* | -36 | 72 |
| IBMETRO* | 28 | 38 |
| LATU* | 26 | 30 |
| INTI* | -75 | 63 |
| INMETRO* | -16 | 22 |
* participants in SIM.M.FF-K4
Pair-wise degrees of equivalence involving CCM.FF-K4 and SIM.M.FF-K4 are given on page 18 of the SIM.M.FF-K4 Final Report.
Results are presented under A4 printable format in Summary Results (.PDF file).
| Metrology area, Sub-field | Mass and related quantities, Fluid Flow |
| Description | Liquid volume |
| Time of measurements | 2007 |
| Status | Approved for equivalence |
| Final Reports of the comparisons | |
| Measurand | Water volume: 100 mL and 20 L |
| Transfer device | One 20 L pipette and several 100 mL glass pycnometers |
| Comparison type | Key Comparison |
| Consultative Committee | CCM (Consultative Committee for Mass and Related Quantities) |
| Conducted by | SIM (Inter-American Metrology System) |
| Comments | SIM.M.FF-K4 results published on 09 January 2010 SIM.M.FF-K4, EURAMET.M.FF-K4.b, and APMP.M.FF-K4 results are linked to those of CCM.FF-K4 for nominal value 20 L SIM.M.FF-K4 results are linked to those of CCM.FF-K4 for nominal value 100 mL (Transfer Standard TS 03.04.04) Liquid volume |
| Pilot institute |
CENAM
Centro Nacional de Metrologia Mexico |
| Contact person | R. Arias +52 442 2110571 |
| Pilot laboratory | |
|---|---|
| CENAM |
Centro Nacional de Metrologia, Mexico, SIM |
| BSJ |
Bureau of Standards Jamaica, Jamaica, SIM |
| CENAMEP AIP |
Centro Nacional de Metrología de Panama AIP, Panama, SIM |
| IBMETRO |
Instituto Boliviano de Metrología, Bolivia, SIM |
| INMETRO |
Instituto Nacional de Metrologia, Qualidade e Tecnologia, Brazil, SIM |
| INTI |
Instituto Nacional de Tecnologia Industrial, Argentina, SIM |
| LACOMET |
Laboratorio Costarricense de Metrologia, Costa Rica, SIM |
| LATU |
Laboratorio Tecnologico del Uruguay, Uruguay, SIM |
| NIST |
National Institute of Standards and Technology, United States, SIM |
This page proposes print-out on A4 paper (portrait) of the comparison details (best printed out using a black and white printer).
Please, select items to be printed out, then click on "OK" :
CCM.FF-K4, EURAMET.M.FF-K4.b, SIM.M.FF-K4, and APMP.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 20 L
THREE TRANSFER STANDARDS
|
For each of the transfer standards, the key comparison reference value, xR, is computed either as the median or as the weighted mean of the results. Its expanded uncertainty UR is approximately given at a 95% level of confidence.
|
|
For each transfer standard, a first degree of equivalence for laboratory i with respect to the key comparison reference value is calculated as a pair of terms, both expressed in relative value: |
| The degree of equivalence between two laboratories i and j is given by a pair of terms, both expressed in relative value: Dij = Di - Dj and its expanded uncertainty Uij at approximately a 95% level of confidence. |
The linking process is described in section 7 of the EURAMET.M.FF-K4.b Final Report. The Matrix of equivalence obtained at 20 L in CCM.FF-K4 is thus extended to EURAMET.M.FF-K4.b participants.
Note: The Dij values given in the Annex 2 of the EURAMET.M.FF-K4.b Final Report correspond to -Dij values shown in the Matrix of equivalence.
The regional comparison reference value is first determined as the median of the SIM results for transfer standard TS 710-05, as described in section 8 of the SIM.M.FF-K4 Final Report.
Then the linking process uses common participation of CENAM, NIST and INMETRO in both key comparisons, as described in section 9 of the same Report.
Pair-wise degrees of equivalence involving CCM.FF-K4 and SIM.M.FF-K4 are given on page 16 of the SIM.M.FF-K4 Final Report.
The linking process uses common participation of NMIA and CENAM in both key comparisons, as described in section 7 of the APMP.M.FF-K4 Final Report.
Pair-wise degrees of equivalence involving APMP.M.FF-K4 participants are given on page 17 of the APMP.M.FF-K4 Final Report.
CCM.FF-K4 and SIM.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 100 mL
TRANSFER STANDARD: TS 03.04.04
| The key comparison reference value, xR, is computed as the median of the results. Its expanded uncertainty UR is approximately given at a 95% level of confidence. The details are explained in Appendix C of the CCM.FF-K4 Final Report. xR = 100.1599 mL and UR = 0.0013 mL |
| The degree of equivalence of laboratory i with respect to the key comparison reference value is given by a pair of terms, both expressed in relative value: Di = (xi - xR)/xR and its expanded uncertainty Ui at approximately a 95% level of confidence. |
| The degree of equivalence between two laboratories i and j is given by a pair of terms, both expressed in relative value: Dij = Di - Dj and its expanded uncertainty Uij at approximately a 95% level of confidence. |
The regional comparison reference value is first determined as the median of the SIM results for transfer standard TS 03.04.04, as described in section 8 of the SIM.M.FF-K4 Final Report.
Then the linking process uses common participation of CENAM and INMETRO in both key comparisons, as described in section 9 of the same Report.
Pair-wise degrees of equivalence involving CCM.FF-K4 and SIM.M.FF-K4 are given on page 18 of the SIM.M.FF-K4 Final Report.
CCM.FF-K4, EURAMET.M.FF-K4.b, SIM.M.FF-K4, and APMP.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 20 L
xi : volume of water the transfer standard is able to deliver after a 60 second period of dripping-off at a reference temperature of 20 °C, measured by laboratory i
ui : standard uncertainty of xi
TRANSFER STANDARD: TS 710-04
| Lab i | xi / mL |
ui / mL |
Date of measurement |
| CENAM | 19 996.71 | 0.17 | Dec 2003 |
| NIST | 19 996.42 | 0.38 | Jan 2004 |
| NRC | 19 996.88 | 0.31 | Mar 2004 |
| SP | 19 992.87 | 0.36 | Apr 2004 |
| PTB | 19 996.80 | 0.20 | Jun 2004 |
| INRIM | 19 997.30 | 0.13 | Aug / Oct 2004 |
| NMIA | 19 996.80 | 0.23 | Oct / Dec 2004 |
| INMETRO | 19 996.77 | 0.15 | Feb 2005 |
TRANSFER STANDARD: TS 710-05
| Lab i | xi / mL |
ui / mL |
Date of measurement |
| CENAM | 19 997.31 | 0.17 | Dec 2003 |
| NIST | 19 996.83 | 0.25 | Jan 2004 |
| NRC | 19 997.75 | 0.31 | Mar 2004 |
| SP | 19 997.40 | 0.36 | Apr 2004 |
| PTB | 19 997.44 | 0.20 | Jun 2004 |
| INRIM | 19 998.00 | 0.15 | Aug / Oct 2004 |
| NMIA | 19 997.16 | 0.22 | Oct / Dec 2004 |
| INMETRO | 19 997.33 | 0.14 | Feb 2005 |
TRANSFER STANDARD: TS 710-06
| Lab i | xi / mL |
ui / mL |
Date of measurement |
| CENAM | 20 005.60 | 0.17 | Dec 2003 |
| NIST | 20 005.04 | 0.37 | Jan 2004 |
| NRC | 20 005.98 | 0.31 | Mar 2004 |
| SP | 20 005.63 | 0.36 | Apr 2004 |
| PTB | 20 005.54 | 0.20 | Jun 2004 |
| INRIM | 20 005.96 | 0.14 | Aug / Oct 2004 |
| NMIA | 20 005.59 | 0.22 | Oct / Dec 2004 |
| INMETRO | 20 005.54 | 0.15 | Feb 2005 |
TRANSFER STANDARD : TS 710-04
xi-EUR.b : volume of water measured by laboratory i participant in EURAMET.M.FF-K4.b
Ui-EUR.b : expanded uncertainty (k = 2) of xi-EUR.b
| Lab i | xi-EUR.b / mL |
Ui-EUR.b / mL |
Date of measurement |
| SP | 20 002.44 | 0.49 | May 07 |
| JV | 20 002.87 | 0.80 | Jul 07 |
| METAS | 20 000.95 | 1.22 | Aug 07 |
| IPQ |
20 002.47 |
0.58 |
Aug 07 |
| VSL |
20 002.07 |
0.70 |
Sep 07 |
| SMU |
20 001.72 |
0.40 |
Sep 07 |
| MKEH |
20 002.32 |
0.36 |
Oct 07 |
| INRIM |
20 002.14 |
0.39 |
Nov 07 |
| PTB |
20 002.04 |
0.39 |
Jan 08 |
| DMDM |
20 002.05 |
0.68 |
Feb 08 |
| UME | 20 002.23 | 0.39 | Feb 08 |
| EIM | 20 001.95 | 0.33 | Mar 08 |
| BEV | 20 002.11 | 0.48 | Apr 08 |
| CMI |
20 000.95 |
1.74 |
Apr 08 |
TRANSFER STANDARD : TS 710-05
xi-SIM : volume of water measured by laboratory i participant in SIM.M.FF-K4
ui-SIM : standard uncertainty of xi-SIM
| Lab i | xi-SIM / mL |
Ui-SIM / mL |
Date of measurement |
| CENAM | 19 995.03 | 0.25 | Jan 07 |
| NIST | 19 995.79 | 0.59 | Mar 07 |
| BSJ | 19 996.62 | 6.40 | Apr 07 |
| LACOMET |
19 990.39 |
1.46 |
Jun 07 |
| CENAMEP |
19 995.47 |
0.53 |
Aug 07 |
| INDECOPI |
19 994.45 |
0.89 |
Oct 07 |
| IBMETRO |
19 994.18 |
0.96 |
Feb 08 |
| LATU |
19 993.50 |
0.59 |
Apr 08 |
| INTI |
19 995.04 |
0.12 |
Aug 08 |
| INMETRO |
19 995.06 |
0.23 |
Oct 08 |
TRANSFER STANDARD : TS 710-04
xi-APMP : volume of water measured by laboratory i participant in APMP.M.FF-K4
Ui-APMP : expanded uncertainty (k = 2, unless otherwise stated) of xi-APMP
| Lab i | xi-APMP / mL |
Ui-APMP / mL |
Date of measurement |
| CENAM | 19 992.94 | 0.65 (k = 2.09) | Jul 06 |
| NMIA | 19 992.87 | 0.44 | Jul - Aug 06 |
| SCL | 19 992.50 | 0.50 | Aug - Sep 06 |
| KRISS |
19 992.87 |
0.44 |
Sep 06 |
| NIM |
19 992.98 |
0.65 (k = 1.96) |
Oct 06 |
| NMISA |
19 991.57 |
2.30 (k = 2.28) |
Nov 06 - Jan 07 |
| NIMT |
19 990.03 |
0.95 |
Jan - Feb 07 |
| NMIJ |
19 993.10 |
2.20 |
Feb - Mar 07 |
| VMI-STAMEQ |
19 992.33 |
0.66 |
Jun 07 |
| MUSSD |
19 993.39 |
0.72 (k = 2.19) |
Jul 07 |
| NMIA | 19 992.85 | 0.44 | Jul - Aug 07 |
CCM.FF-K4 and SIM.M.FF-K4
MEASURAND: Volume
NOMINAL VALUE: 100 mL
TRANSFER STANDARD: TS 03.04.04
xi : volume of water the transfer standard contains at a reference temperature of
20 °C, measured by laboratory i
ui : standard uncertainty of xi
| Lab i | xi / mL |
ui / mL |
Date of measurement |
| CENAM | 100.159 4 | 0.000 87 | Dec 2003 |
| NRC | 100.163 6 | 0.000 75 | Mar 2004 |
| SP | 100.161 2 | 0.001 6 | Apr 2004 |
| INRIM | 100.157 8 | 0.000 84 | Aug / Oct 2004 |
| NMIA | 100.160 9 | 0.001 1 | Oct / Dec 2004 |
| INMETRO | 100.158 5 | 0.000 72 | Feb 2005 |
During the comparison, three transfer standards were used, but one of the pycnometers (serial 03.04.15) suffered an irreversible damage; this occurred after INDECOPI tests. Therefore, pycnometer 03.01.15 was tested by CENAM, BSJ, LACOMET, CENAMEP AIP and INDECOPI. This transfer standard was then replaced by pycnometer 03.01.17, which was measured by CENAM, IBMETRO, LATU, INTI and INMETRO.
Degrees of equivalence are computed using results from pycnometer 03.04.04, as it is the only artefact measured by all participants. Only results obtained with this transfer standard are reported here.
MEASURAND: Volume
NOMINAL VALUE: 100 mL
TRANSFER STANDARD: TS 03.04.04
xi-SIM : volume of water measured by laboratory i participant in SIM.M.FF-K4
ui-SIM : standard uncertainty of xi-SIM
| Lab i | xi-SIM / mL |
ui-SIM / mL |
Date of measurement |
| CENAM | 99.080 2 | 0.001 6 | Jan 2007 |
| BSJ | 100.130 7 | 0.037 | Apr 2007 |
| LACOMET | 99.081 8 | 0.003 1 | Jun 2007 |
| CENAMEP | 99.079 0 | 0.001 4 | Aug 2007 |
| INDECOPI | 99.076 9 | 0.003 5 | Oct 2007 |
| IBMETRO |
99.083 3 |
0.001 7 |
Feb 2008 |
| LATU |
99.083 1 |
0.001 3 |
Apr 2008 |
| INTI |
99.073 0 |
0.003 0 |
Aug 2008 |
| INMETRO | 99.078 9 | 0.000 95 | Oct 2008 |
