CCQM-K158

MEASURAND   Copper in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Copper in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Mercury in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 5 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Mercury in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

 

Enlarged graph
Graph_Hg_CCQM-K158

CCQM-K158

MEASURAND   Potassium in polished rice flour

NOMINAL VALUE 100 mg/kg - 1000 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Potassium in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Sodium in polished rice flour

NOMINAL VALUE 2 mg/kg - 10 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Sodium in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Lead in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 1 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Lead in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Antimony in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Antimony in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Total arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Total arsenic in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Inorganic arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

Degrees of equivalence represented by Di = (xI - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Inorganic arsenic in rice flour
Di / mg/kg
Participating institutes

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Copper in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
NIS* -0.406 0.213
INTI* -0.291 0.229
NIMT -0.023 0.072
HSA 0.007 0.070
KRISS 0.0188 0.0625
NMIJ 0.029 0.070
LATU 0.036 0.072
NMISA 0.040 0.089
MIRS/IJS/F-2,O-2 0.145 0.156
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Mercury in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 5 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
INTI -0.040 0.080
MIRS/IJS/F-2,O-2 -0.038 0.040
NMISA* -0.023 0.040
GL -0.005 0.028
NMIA -0.001 0.024
NIM 0.0042 0.0172
HSA 0.0050 0.0137
LATU 0.0122 0.0205
NIMT* 0.0182 0.0398
KRISS* 0.0228 0.0396
NIS* 0.6372 0.0831
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Potassium in polished rice flour

NOMINAL VALUE 100 mg/kg - 1000 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
NIMT* -72.6 43.5
NIS -70.7 77.9
NMISA* -28.6 25.2
MIRS/IJS/F-2,O-2 -20.6 34.1
PTB -2.3 6.7
KRISS 2.0 4.2
INM (CO) 5.2 23.6
NMIJ 5.6 15.2
LATU 10.4 14.6
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Sodium in polished rice flour

NOMINAL VALUE 2 mg/kg - 10 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
NIS* -1.74 0.27
MIRS/IJS/F-2,O-2 -0.15 0.29
KRISS -0.02 0.33
NMIJ 0.031 0.162
NMISA 0.05 0.24
NIMT* 3.35 0.87
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Lead in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 1 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
NMISA* -0.0596 0.0372
INM (CO)* -0.0336 0.0460
METAS* -0.0186 0.0382
MIRS/IJS/F-2,O-2 -0.0126 0.0154
GL -0.0016 0.0099
NMIJ -0.0016 0.0085
NIMT -0.0016 0.0085
HSA 0.0004 0.0105
LATU 0.0014 0.0085
KRISS 0.0024 0.0109
PTB 0.0024 0.0073
NIS 0.0034 0.0379
NIM 0.0044 0.0072
NMIA* 0.0134 0.0383
INTI* 0.0254 0.0412
INMETRO* 0.0284 0.0386
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Antimony in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
NIMT* -0.0743 0.0425
MIRS/IJS/F-2,O-2* -0.0673 0.0638
INTI -0.0143 0.0725
GL -0.0063 0.0358
NMIA -0.0023 0.0340
KRISS -0.0017 0.0081
HSA 0.0037 0.0332
NMIJ 0.0084 0.0114
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Total arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

Degrees of equivalence represented by Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
NIMT* -0.0134 0.0041
METAS* -0.0094 0.0060
MIRS/IJS/F-2,O-2 -0.0027 0.0072
LGC -0.0010 0.0027
NIM -0.0004 0.0042
NMIJ -0.0001 0.0041
NMIA 0.0003 0.0058
KRISS 0.0006 0.0139
LATU 0.0006 0.0041
HSA 0.0008 0.0040
NRC 0.0011 0.0040
GL 0.0016 0.0055
INTI 0.0030 0.0114
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

CCQM-K158

MEASURAND   Inorganic arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

Degrees of equivalence represented by Di = (xI - xR) and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
NRC* -0.0290 0.0206
NIMT* -0.0093 0.0224
GL -0.0014 0.0076
HSA -0.0007 0.0058
LGC -0.0003 0.0035
NMIJ 0.0004 0.0023
NIM 0.0036 0.0032
Participating institutes
CCQM-K158

*Ui  for this participant was estimated after summing in quadrature the participant's reported uncertainty value and the dark uncertainty (tau) associated with the key comparison reference value (KCRV) because estimation using the reported uncertainty value alone results in nonequivalence with the KCRV.

Comparison
Comparison close
CC comparison
Linked comparison
CCQM-K158
Metrology area, Sub-field Chemistry and Biology, Inorganics
Description Elements and inorganic arsenic in rice flour
Time of measurements 2021 - 2022
Status Approved for equivalence
Final Reports of the comparisons
Measurand Mass fraction of Cu, Hg, K, Na, Sb or Pb in rice flour
Mass fraction of total arsenic and inorganic arsenic in rice flour

Transfer device Sample A: 10 g sample in an amber glass bottle (two bottles)
Sample B: 10 g sample in an amber glass bottle (one bottle)
Comparison type Key Comparison
Consultative Committee CCQM (Consultative Committee for Amount of Substance)
Conducted by CCQM (Consultative Committee for Amount of Substance)
Comments This study has two parts:
Part A which covers the trace elements measurement analysis without arsenic.
Part B which covers the measurement analysis of total arsenic and inorganic arsenic.
Pilot institute NMIJ AIST
National Metrology Institute of Japan
Japan
Contact person Kazumi Inagaki

Additional
First Name Last Name
wwww@ww.www +356719836 Institute 1 Institute 1 Khmelnitskiy
Pilot laboratory
NMIJ AIST

National Metrology Institute of Japan, Japan, APMP

GL

Government Laboratory, Hong Kong, China, APMP

HSA

Health Science Authority, Singapore, APMP

INM (CO)

Instituto Nacional de Metrología de Colombia, Colombia, SIM

INMETRO

Instituto Nacional de Metrologia, Qualidade e Tecnologia, Brazil, SIM

INTI

Instituto Nacional de Tecnologia Industrial, Argentina, SIM

KRISS

Korea Research Institute of Standards and Science, Korea, Republic of, APMP

LATU

Laboratorio Tecnologico del Uruguay, Uruguay, SIM

LGC

Laboratory of the Government Chemist, United Kingdom, EURAMET

METAS

Federal Institute of Metrology, Switzerland, EURAMET

MIRS/IJS/F-2,O-2

MIRS/Jozef Stefan Institute/Low and Medium Energy Physics F2, Environmental Sciences O2, Slovenia, EURAMET

NIM

National Institute of Metrology, China, APMP

NIMT

National Institute of Metrology (Thailand), Thailand, APMP

NIS

National Institute for Standards, Egypt, AFRIMETS

NMIA

National Measurement Institute, Australia, Australia, APMP

NMISA

National Metrology Institute of South Africa, South Africa, AFRIMETS

NRC

National Research Council, Canada, SIM

PTB

Physikalisch-Technische Bundesanstalt, Germany, EURAMET

CCQM-K158

MEASURAND   Copper in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on page 23 of the CCQM-K158 final report. The reported result for NIS was not included in the calculation of xR.

 

        xR = 1.345 mg/kg     uR = 0.0030 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 27 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Mercury in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 5 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on page 23 of the CCQM-K158 final report. The reported result for NIS was not included in the calculation of xR.

 

        xR = 0.4788 mg/kg     uR = 0.0059 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 27 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Potassium in polished rice flour

NOMINAL VALUE 100 mg/kg - 1000 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on page 23 of the CCQM-K158 final report. The reported result for NIMT and NIS were not included in the calculation of xR.

 

        xR = 616.6 mg/kg     uR = 3.3 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 27 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Sodium in polished rice flour

NOMINAL VALUE 2 mg/kg - 10 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on page 23 of the CCQM-K158 final report. The reported result for NIS and NIMT were not included in the calculation of xR.

 

        xR = 5.399 mg/kg     uR = 0.064 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 27 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Lead in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 1 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on page 23 of the CCQM-K158 final report.

 

        xR = 0.2166 mg/kg     uR = 0.0030 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 27 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Antimony in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on page 23 of the CCQM-K158 final report. The reported result for NIMT was not included in the calculation of xR.

 

        xR = 1.0130 mg/kg     uR = 0.0050 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 27 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Total arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on pages 50 and 51 of the CCQM-K158 final report. The reported result for NIMT and METAS were not included in the calculation of xR.

 

        xR = 0.1064 mg/kg     uR = 0.0006 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 54 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Inorganic arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR were calculated using the Adaptive Weighted Average statistical model following the NIST Decision Tree, as explained on pages 50 and 51 of the CCQM-K158 final report. The reported result for NRC and NIMT were not included in the calculation of xR.

 

        xR = 0.0903 mg/kg     uR = 0.0006 mg/kg

 

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence is calculated as explained on page 54 of the CCQM-K158 final report.

CCQM-K158

MEASURAND   Copper in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  NIS* 0.939 0.088#
  INTI 1.054 0.097#
  NIMT 1.322 0.020
  HSA 1.352 0.015
  KRISS 1.3640 0.0062
  NMIJ 1.3740 0.018
  LATU 1.381 0.020
  NMISA 1.385 0.033
  MIRS/IJS/F-2,O-2 1.490 0.060

 

* Reported value is not included for the calculation of the key comparison reference value

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature

CCQM-K158

MEASURAND   Mercury in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 5 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  INTI 0.439 0.040
  MIRS/IJS/F-2,O-2 0.441 0.015
  NMISA 0.456 0.017#
  GL 0.474 0.013
  NMIA 0.478 0.010
  NIM 0.4830 0.0064
  HSA 0.4838 0.0032
  LATU 0.4910 0.008
  NIMT 0.4970 0.0171#
  KRISS 0.5016 0.0169#
  NIS* 1.116 0.0409#

 

* Reported value is not included for the calculation of the key comparison reference value

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature

CCQM-K158

MEASURAND   Potassium in polished rice flour

NOMINAL VALUE 100 mg/kg - 1000 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  NIMT* 539 22#
  NIS* 541 40
  NMISA 583 13#
  MIRS/IJS/F-2,O-2 591 18
  PTB 609.3 3.9
  KRISS 613.6 1.9
  INM (CO) 617 12
  NMIJ 617.2 8.2
  LATU 622.0 7.8

 

* Reported value is not included for the calculation of the key comparison reference value 

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature

CCQM-K158

MEASURAND   Sodium in polished rice flour

NOMINAL VALUE 2 mg/kg - 10 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  NIS* 3.66 0.12#
  MIRS/IJS/F-2,O-2 5.25 0.16
  KRISS 5.38 0.18
  NMIJ 5.431 0.090
  NMISA 5.45 0.14
  NIMT* 8.75 0.44#

 

* Reported value is not included for the calculation of the key comparison reference value

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature

CCQM-K158

MEASURAND   Lead in polished rice flour

NOMINAL VALUE 0.1 mg/kg - 1 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  NMISA 0.1570 0.0170#
  INM (CO) 0.183 0.022#
  METAS 0.198 0.018#
  MIRS/IJS/F-2,O-2 0.204 0.006
  GL 0.2146 0.0045
  NMIJ 0.2146 0.0028
  NIMT 0.215 0.003
  HSA 0.2168 0.0043
  LATU 0.2181 0.0033
  KRISS 0.2186 0.0033
  PTB 0.2189 0.0022
  NIS 0.220 0.019
  NIM 0.221 0.002
  NMIA 0.2305 0.0173#
  INTI 0.2415 0.019#
  INMETRO 0.2448 0.0175#

 

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature

CCQM-K158

MEASURAND   Antimony in polished rice flour

NOMINAL VALUE 0.5 mg/kg - 5 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  NIMT* 0.939 0.021#
  MIRS/IJS/F-2,O-2 0.946 0.033#
  INTI 0.999 0.038
  GL 1.007 0.019
  NMIA 1.011 0.018
  KRISS 1.0115 0.0038
  HSA 1.017 0.018
  NMIJ 1.0217 0.0066

 

* Reported value is not included for the calculation of the key comparison reference value

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature

CCQM-K158

MEASURAND   Total arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  NIMT* 0.093 0.004#
  METAS* 0.0970 0.0050#
  MIRS/IJS/F-2,O-2 0.1037 0.0037
  LGC 0.1053 0.0012
  NIM 0.1060 0.0020
  NMIJ 0.1063 0.0020
  NMIA 0.1067 0.0029
  KRISS 0.107 0.007
  LATU 0.1070 0.0019
  HSA 0.1072 0.0019
  NRC 0.1075 0.0020
  GL 0.1080 0.0027
  INTI 0.1094 0.0057

 

* Reported value is not included for the calculation of the key comparison reference value

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature

CCQM-K158

MEASURAND   Inorganic arsenic in polished rice flour

NOMINAL VALUE > 0.02 mg/kg

 

xi   measured mass fraction reported by laboratory iLabi

ui   combined standard uncertainty of xi

 

  Labi xi ui
  mg/kg mg/kg
  NRC* 0.0613 0.0103#
  NIMT* 0.0810 0112#
  GL 0.0889 0.0039
  HSA 0.0896 0.0029
  LGC 0.0901 0.0016
  NMIJ 0.09070 0.00096
  NIM 0.0939 0.0015

 

* Reported value is not included for the calculation of the key comparison reference value

# Participant's value includes the uncertainty and the dark uncertainty, τ, summed in quadrature